4-(4-Bromo­phen­yl)-2,6-diphenyl­pyridine

نویسندگان

  • Qun Cao
  • Yu Xie
  • Jie Jia
  • Xiao-Wei Hong
چکیده

In the title compound, C(23)H(16)BrN, the three benzene rings show a disrotatory counter-rotating arrangement around the central pyridine ring and are twisted with respect to the pyridine ring with dihedral angles of 19.56 (13), 27.54 (13) and 30.51 (13)°.

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منابع مشابه

4-(4-Chloro­phen­yl)-2,6-diphenyl­pyridine

In the title compound, C(23)H(16)ClN, the crystal packing exhibits no significantly short inter-molecular contacts. The benzene rings show a disrotatory arrangement and the angles between them and the pyridine ring range from 20.80 (3) to 37.56 (4)°. The Cl atom deviates by 0.01 (3) Å from the plane of the benzene ring to which it is attached.

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{2,6-Bis[(4-bromo­phen­yl)imino­meth­yl]pyridine-κ3 N,N′,N′′}trichlorido­chromium(III)

In the title compound, [CrCl(3)(C(19)H(13)Br(2)N(3))], the Cr(3+ )ion is coordinated by the tridentate 2,6-bis-[(4-bromo-phen-yl)imino-meth-yl]pyridine Schiff base ligand in a fac-octa-hedral geometry. The dihedral angles between the pyridine and benzene rings are 23.9 (6) and 70.7 (1)°.

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rac-2,2′-(Thiane-2,6-di­yl)bis­[1-(4-bromo­phen­yl)ethanone]

In the title compound, C(21)H(20)Br(2)O(2)S, prepared by the reaction of 1,9-bis-(4-bromo-phen-yl)nona-2,7-diene-1,9-dione with sodium sulfide nona-hydrate in acetonitrile, the six-membered thio-pyran ring has a chair conformation while the H atoms ortho to the S atom adopt a cis configuration. The dihedral angle between the two benzene rings is 2.59 (8)°.

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2-(4-Bromo­phen­yl)-N-(2,6-dimethyl­phen­yl)acetamide

In the title compound, C(16)H(16)BrNO, the dihedral angle between the benzene rings is 69.8 (2)°. In the crystal, N-H⋯O hydrogen bonds link the mol-ecules into C(4) chains propagating in [100]. Adjacent mol-ecules in the chains are also linked by C-H⋯O inter-actions which, along with the N-H⋯O hydrogen bonds, generate R(2) (1)(6) loops.

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N,N′-Bis(4-bromo­phen­yl)pyridine-2,6-dicarboxamide

The mol-ecule of the title compound, C19H13Br2N3O2, lies about a twofold rotation axis. The benzene ring makes dihedral angles of 8.9 (2) and 16.4 (2)° with the central pyridine ring and the second benzene ring, respectively. An intra-molecular N-H⋯N contact occurs. In the crystal, mol-ecules are connected by pairs of N-H⋯O hydrogen bonds into chains along the c axis.

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عنوان ژورنال:

دوره 65  شماره 

صفحات  -

تاریخ انتشار 2009